SEC-RI-UV-MALLS with eluent 0.5% LiBr in DMSO.
Instrument resposibles run the instrument. Other users ask the instrument responsibles about when it is possible to run and prepare the samples for the instrument responsibles to start the run.
Responsible: Nikola Krivánková nikolakr@kth.se, Tijana Todorovic tijanat@kth.se
Usual preparation:
Mix 4 mg sample in 2 ml eluent (0.5%LiBr+DMSO). Dissolve at 60C over night. Filter with 0.45um syringe filter into glass vial.